Title Hydrothermal synthesis, characterization and optical properties of 3D flower like indium sulfide nanostructures
Author: Abadi, Parvaneh Ghaderi Sheikhi; Salavati-Niasari, Masoud & Davar, Fatemeh
Superlattices and Microstructures, 2013
2013
http://www.sciencedirect.com/science/article/pii/S0749603612002601
More details: High-quality and high-yield 3D flower like indium sulfide (In2S3) nanostructures with cubic structure were synthesized by a wet chemical route, without using any surfactant and organic solvents at 160\&\#xa0;??C for 12\&\#xa0;h, by using InCl3 and 2-aminothiophenol (2-ATP) as starting reagents. The obtained In2S3 with different morphologies and size was characterized by X-ray diffraction pattern (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FT-IR), and ultraviolet?��visible (UV?��vis) spectroscopy. The effects of reaction parameters, such as temperature, precursor concentration and reaction time on the morphology, and particle size of products were investigated. Our experimental results showed that temperature and time reaction played key roles in the final morphology of In2S3. The morphology of In2S3 structures could be changed from one-dimensional (1D) structures to three-dimensional (3D) structures by increasing reaction time to 24\&\#xa0;h. In the present study the optical properties 3D In2S3 structures were investigated. 3D structure,Hydrothermal,Indium sulfide,Nanostructure,Semiconductor
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